WS 2016 SS 2016
WS 2015
WS 2014 SS 2015
Department of Chemistry
open physics
KVL / Klausuren / MAP 1st HS: 12.10  2nd HS: 07.12  sem.br.: 15.02  begin SS: 17.04

2020155188 NMR spectroscopy (1st HS)  VVZ 

VL
Mon 11-13
weekly NEW 14 1'15 (60) Clemens Mügge
Tue 15-17
weekly NEW 14 0'07 (120)
SE
Mon 15-17
weekly NEW 14 0'06 (149) Clemens Mügge

Digital- & Präsenz-basierter Kurs

Aims
1.Basic understandig of NMR experiment:
Principle of method, instrumentation, NMR spectrum.

2.Spectrum analysis and interpretation:
Identification of spectral data and transformation in structure information (constitution, configuration,conformation).

3.Modern NMR techniques: 1D,2D,nD.

4.Knowledge of applications of NMR
Requirements
erfolgreicher Abschluss des Moduls AU2
Structure / topics / contents
1.Physical basics:
Nuclear magnetism,nuclear magnetic resonance, relaxation.
2.Instrumentation:
PFT technique,Equipment configuration,magnet system, transmitter, receiver, quality criteria.
3.NMR spectrum and spectral parameters:
chemical shifts, coupling constants,signal intensity,LB,T1,NOE's.
4.Spectrum analysis and interpretation:
1H,13C,19F,31P spectra,spectrum analysis algorithm.
5.1D,2D,nD NMR techniques:
COSY,TOCSY,NOESY,EXSY,HMQC,HMBC,1D-COSY,...
6.Applications:
Org. and inorg.chemistry, bio-,enviromental and food chemistry, medicine
Assigned modules
17/AU5 / (AU3 SO 2009)
Amount, credit points; Exam / major course assessment
0 SWS, 0 SP/ECTS (Arbeitsanteil im Modul für diese Lehrveranstaltung, nicht verbindlich)
Written examination about NMR lecture and tutorials,
60 min.

Weighting examinations: NMR / IR / MS = 1 / 1 / 1
Contact
Clemens Mügge
Literature
H.Günther. NMR Spectroscopy. Wiley-VCH, 2013
H.Friebolin. Ein- und zweidimensionale NMR-Spektroskopie. Wiley-VCH
S.Berger. 200 and more NMR experiments. Wiley-VCH
M.Hesse,H.Meier,B.Zeeh. Spektroskopische Methoden in der organischen Chemie. Georg Thieme
R.Meusinger. NMR-Spektren richtig ausgewertet. Springer
T.N.Mitchell, B. Costicella. NMR-From Spectra to Structures. Springer
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